How the Oil Analysis
Program (OAP) Works
OAP is a 4-step process:
(1)
Registration
(2) Sampling
(3) Analysis
(4) Diagnostic Reporting
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Note: We do not test any
aircraft/aviation oils.
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Step 1 - Registration
1. Begin the OAP process by purchasing a
sampling kit. Simply call Oil Analyzers Inc. at (715) 395-0222
for pricing information or to order kits (and a sample pump if
desired). You may purchase kits singly or in quantities of 10,
25, 50 or 100, with lower per-kit prices for larger orders.
2. Upon receipt of your order, OAI will
immediately send out your sample kit, which includes sample
container, sample information form, mailer and complete sampling
and mailing instructions.
Step 2 - Sampling
1. Read the Oil Sampling Procedures
included in the kit.
2. Fill out the Sample Information Form
completely.
3. Take a sample (minimum: 2 to 3 oz)
using the convenient instructions included in your kit.
4. Close and seal sample container tightly.
5. Using the mailing instructions included
in your kit, send the filled sample container and the Sample
Information Form to OAI in the supplied mailer.
Step 3 - Analysis
Upon receipt of your sample at the Oil
Analyzers Inc. laboratory, all requisite testing will be
performed. All analyses include determination of viscosity, fuel
dilution (if applicable), water, dirt content, fuel soot
contamination (if applicable), plus spectrochemical analysis for
21 trace elements to determine component wear, airborne dirt,
anti-freeze contamination (if applicable), and oil additive
concentrations.
The analyses also included a neutralization
value determination - Total Base Number, TBN (primarily for
gasoline and diesel motor oils) or Total Acid Number, TAN
(non-crankcase lubricants). Oxidation values and nitration value
(if applicable) are also determined
Step 4 - Reporting
1. OAI will mail your analysis report to
you the day your sample is analyzed. For even faster results,
simply request on the Sample Information Form that your report
be faxed to you. Be sure to include your fax number.
2. If your analysis uncovers a critical
problem, such as pending equipment failure, a technician will
telephone you directly to advise you of the situation and
recommend a course of corrective action.
The Sampling Process
Trend Analysis
A single sampling analysis is useful in
providing information when critical failure conditions exist.
However, trend analysis is a better tool for estimating the useful
life or overall condition of your engine or equipment. Trend
analysis samples are taken and analyzed at regularly scheduled
intervals. Comparing the most recent analysis to previous reports
on a given machine shows the development of trends. Monitoring
these trends enables early detection of internal abnormalities.
Tested values falling within acceptable limits may show a pattern
of subtle variance, which could signal a developing problem.
Machines of the same type will accumulate
contaminants and wear at different rates. Performing trend
analysis on each machine is the most effective method of giving
you an internal look at your equipment and enabling you to deal
with developing problems before they become catastrophic
situations.
Sampling Frequency
The frequency of sample analysis from your
equipment depends on the machine type, machine application and
condition, operating environment and other variables. For example,
many machines that operate in harsh environments, such as heavy
equipment in mining or construction, require short oil sampling
intervals - every 100 to 300 operating hours. However, certain
power transmission systems, such as gearboxes and hydraulic
systems used inside manufacturing and production facilities,
require no more than quarterly sampling intervals. The following
table lists generic sampling frequencies for common equipment
types, and is provided as a guideline only. Additional information
is available from Oil Analyzers Inc., your lubricant supplier, and
the equipment manufacturer.
Collecting a clean and representative oil
sample is critical to the oil analysis process. Put simply, an oil
analysis is only as good as the sample taken. The accuracy and
reliability of the data produced by an analysis hinges on
receiving a representative sample from the equipment to be tested.
To assure that the sample extracted is representative of the
system, always follow proper sampling procedures.
| EQUIPMENT
TYPE |
TEST
PACKAGE |
RECOMMENDED
SAMPLING FREQUENCY |
| MOTOR
VEHICLES |
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| Diesel
engines |
Basic
with TBN |
100
- 500 hours, 3500 - 20,000 miles |
| Gasoline
engines |
Basic
with TBN |
50
- 200 hours, 2000 - 7500 miles |
| Transmissions |
Basic
with TAN |
30,000
- 100,000 miles |
| Gears,
differentials, final drives |
Basic
with TAN |
30,000
- 100,000 miles |
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| INDUSTRIAL |
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Normal Use Intermittent
Use |
| Hydraulics |
Basic
with TAN |
750
hours or monthly Quarterly |
| Gas
turbines |
Basic
with TAN |
750
hours or monthly Quarterly |
| Steam
turbines |
Basic
with TAN |
1500
hours or bimonthly Quarterly |
| Air
or gas compressors |
Basic
with TAN |
750
hours or monthly Quarterly |
| Refrigeration
compressors |
Basic
with TAN |
Quarterly |
| Natural
gas engines |
Basic
with TAN |
750
hours or monthly |
| Gears
and bearings (industrial) |
Basic
with TAN |
1500
hours or bimonthly Quarterly |
SAMPLING METHODS
1. The component sampled should be brought
to operating temperature prior to sampling. This will assure that
the insoluble and semi-soluble material is suspended evenly
throughout the system. Samples taken from components that have
been inactive for long periods are not representative.
2. Sample should always be taken in the same
manner and from the same point.
3. Do not sample a component directly after
an oil change or after a large amount of makeup oil has been
added.
4. Use a clean, dry, unbreakable container.
Never reuse containers or sampling tubing.
Collect your sample using one of the three
following methods:
1. Sample Pump Method
Purchase a sample pump when ordering your
sample kit. The pump will come with complete instructions and
will enable you to draw a sample quickly and easily. Seal the
bottle tightly.
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| G-1206 Oil Suction
Pump with 10-foot hose |
2. Sample Valve/Petcock Method
The valve should be wiped clean and any
stagnant oil should be drained prior to catching a sample run.
Seal the bottle tightly. Wipe bottle clean.
3. Oil Drain Method
Clean the area around the drain plug
thoroughly to avoid sample contamination. Allow oil to drain for
three to five seconds prior to catching a sample. Place a clean,
dry sample bottle in the oil stream and fill to within 1/2 inch
of the top. Seal bottle tightly. Wipe bottle clean.
SAMPLING TIPS
- For best results, oil samples should be
taken immediately after equipment shutdown, while the
equipment is still at operating temperature. Never sample a
cold engine and always make sure the oil has been well
circulated before taking a sample. Dirt, water and other
debris tend to settle to the bottom of the reservoir while
light fuels tend to float. This separation will compromise
your analysis.
- Good locations for sampling include an
oil gallery, the engine crankcase, the drain plug or dipstick
tube and the equipment reservoir or sump.
- When taking oil from industrial machinery
through a bottom drain, be careful to draw oil until your
sample has a uniform, representative appearance.
- Use samples from the drain pan or oil
filter only as a last resort. For a failed engine that has had
the oil drained, a drain pan or oil filter sample may help
detect the cause of the failure.
- Avoid prolonged skin contact with used
oil. Wash exposed skin with soap and water after exposure.
CAUTION
Engine crankcase oil
temperatures can exceed 200°F. To avoid personal injury, use
protective equipment such as gloves, safety glasses and protective
clothing.
SPECIAL
TESTS AVAILABLE
| Tests |
Lube Tested
|
Method
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Qty Req'd
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| Cloud
point |
Diesel
Fuel |
ASTM
D 2500 |
2
oz |
| Cold
Cranking Simulator |
Engine
Oil |
ASTM
D 5293 |
1
oz |
| Color Test |
Any |
ASTM
D 1500 |
2
oz |
| Cone
Penetration of Lubricating Grease |
Grease |
ASTM
D 217 |
1
lb |
| Corrosion,
Copper Strip |
Any |
ASTM
D 130 |
2
oz |
| Density |
Any |
ASTM
D 1298 |
1
qt |
| Falex Pin
& V-Block Test; per run |
Gear
Lube |
ASTM
D 3233 |
4
oz |
| Flash and
Fire Point - (COC) Cleveland Open Cup |
Any |
ASTM
D 92 |
3
oz |
| Flash
Point - (PMCC) Pensky-Marten Closed Cup |
Any |
ASTM
D 93 |
3
oz |
| Foam
Stability Sequences I, II, III |
Any |
ASTM
D 892 |
1
qt |
| *Fuel
Dilution, % |
Engine
Oil |
FTIR |
1
oz |
| *Fuel
Soot, % |
Engine
Oil |
FTIR |
1
oz |
| Four-Ball
Wear Characteristics |
Any |
ASTM
D 4172 |
4
oz |
| *FTIR
Infrared Analysis |
Any |
FTIR
- Scan |
1
oz |
| Glycol
Base Anti-Freeze Determination in Oils |
Engine
Oil |
ASTM
D 2982 |
1
oz |
| *Metals
Analysis |
Any |
ICP |
1
oz |
| **Neutralization
Number - Total Acid Number |
Any |
ASTM
D 664 |
1
oz |
| **Neutralization
Number - Total Base Number |
Any |
ASTM
D 2896 |
1
oz |
| *Nitration,
% |
Engine
Oil |
FTIR |
1
oz |
| NOACK
Volatility, % Weight Loss |
Engine
Oil |
DIN
51581 |
4
oz |
| *Oxidation,
% |
Any |
FTIR |
1
oz |
| pH Range |
Any |
|
1
oz |
| Pour Point |
Any |
ASTM
D 97 |
4
oz |
| Refractive
Index |
Any |
|
1
oz |
| *Viscosity,
measured in cSt, specify temperature |
Any |
ASTM
D 445 |
2
oz |
| Viscosity
Index (Includes 100°C & 40°C Viscosities) |
Any |
ASTM
D 2270 |
4
oz |
| Water by
Distillation |
Any |
ASTM
D 95 |
2
oz |
| Water by
Mobil Crackle Test |
Any |
MOBIL |
2
oz |
| Water by
Karl Fisher |
Any |
ASTM
D 1123 |
1
oz |
| Water
Separability - Petroleum Oils and Syn. Fluids |
Any |
ASTM
D 1401 |
4
oz |
| *Also
included in standard test package |
| **TAN
or TBN included in standard test package |
| Other
special tests available upon request |
Click HERE
for prices
For Additional Information:
Oil Analyzers, Inc. 2206 Winter St., Superior, WI 54880
(715) 395-0222 - phone/fax
E-Mail Contact: dhorn@oaitesting.com
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